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会员 Pyrrolic and Pyridinic Nitrogen-Rich Carbon Microspheres Derived from Polydopamine as Advanced Anodes for Sodium Ion Batteries
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  • 2024/01/01
  • 作者:
    Hongwei Tao  , Zhengyou He  , Haitao Hu  
  • 页数:
    8
  • 页码:
    1794 - 1801
  • 资源:
  • 文件大小:
    8.41M
摘要
Nitrogen-doped carbon microspheres (NCS) were synthesized via a green and convenient high-temperature pyrolysis of polydopamine. The nitrogen doping content and configuration were precisely adjusted by controlling the pyrolysis temperature. Leveraging the unique spherical morphology and abundant pyridinic-N and pyrrolic-N dopants, the resulting NCS, post-treated at 1000°C, showcases superior electrochemical performance. This includes an outstanding initial Coulombic efficiency (ICE) of 73.4%, remarkable reversible capacity of 386.6 mAh g⁻¹, impressive rate capability reaching 180.1 mAh g⁻¹ at 10 A g⁻¹, and unmatched cycling durability with 75.3% capacity retention after 1500 cycles. The substantial electrostatic repulsion facilitated by densely distributed pyrrolic-N atoms effectively expands the carbon interlayer spacing, ensuring efficient and reversible sodium ion intercalation and deintercalation. The abundant pyrrolic-N and pyridinic-N doping significantly augment surface defect density, facilitating rapid electron/ion transport. Furthermore, the low surface area characteristic of the spherical morphology mitigates irreversible sodium ion consumption during the initial solid electrolyte interface (SEI) formation, guaranteeing a high Coulombic efficiency of the electrode. This study presents a novel avenue for the practical design of hard carbon electrodes.
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